Crystal structure of 1,3-bis(2,3-dimethylquinoxalin-6-yl)benzene

Charles E. Diesendruck, Gabrielle Rubin, Jeffery A. Bertke, Danielle L. Gray, Jeffrey S. Moore

Research output: Contribution to journalArticlepeer-review

Abstract

The title compound, C26H22N4 (I), was synthesized by C - H iridium-catalyzed borylation followed by Suzuki coupling. The molecular structure of (I) consists of a central benzene ring with 3-dimethylquinoxalin-6-yl groups at the 1 and 3 positions. These 2,3-dimethylquinoxalin-6-yl groups twist significantly out of the plane of the benzene ring. There are intermolecular π-π interactions which result in a two-dimensional extended structure. The layers extend parallel to the ab plane and stack along the c axis.

Original languageEnglish
Pages (from-to)1429-1432
Number of pages4
JournalActa Crystallographica Section E: Crystallographic Communications
Volume71
DOIs
StatePublished - 1 Jan 2015
Externally publishedYes

Keywords

  • Suzuki coupling
  • crystal structure
  • iridium catalyzed
  • quionoxaline

ASJC Scopus subject areas

  • General Chemistry
  • General Materials Science
  • Condensed Matter Physics

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