Extraction of humic substances from fresh waters on solid-phase cartridges and their study by Fourier transform ion cyclotron resonance mass spectrometry

A. Ya Zherebker; I. V. Perminova; A. I. Konstantinov; A. B. Volikov; Yu I. Kostyukevich; A. S. Kononikhin; E. N. Nikolaev

doi:10.1134/S1061934816040109

Extraction of humic substances from fresh waters on solid-phase cartridges and their study by Fourier transform ion cyclotron resonance mass spectrometry

A. Ya Zherebker, I. V. Perminova, A. I. Konstantinov, A. B. Volikov, Yu I. Kostyukevich, A. S. Kononikhin, E. N. Nikolaev

Research output: Contribution to journal › Article › peer-review

19 Scopus citations

Abstract

Humic substances (HS) have been extracted from fresh waters on macroporous adsorbents of different types, Amberlite XAD-8 resin and Bond Elute PPL solid-phase cartridge. Comparative analysis of the extracted samples by ultra-high resolution mass spectrometry demonstrated selectivity of the selected adsorbents to the components of the molecular assembly of HS: the XAD-8 resin has affinity to the higher oxidized aromatic compounds and PPL has affinity to substances of stronger aliphatic character and nitrogen-containing compounds. Because of this fact, a comparison of the molecular composition of HS isolated from various sources must be performed taking into account selective adsorption; therefore, it is necessary to compare the products extracted by the same adsorbent for correct interpretation.

Original language	English
Pages (from-to)	372-378
Number of pages	7
Journal	Journal of Analytical Chemistry
Volume	71
Issue number	4
DOIs	https://doi.org/10.1134/S1061934816040109
State	Published - 1 Apr 2016
Externally published	Yes

Keywords

Fourier transform mass spectrometry
XAD-8
extraction
fresh water
humic substances
selective adsorption
solid-phase cartridge

ASJC Scopus subject areas

Analytical Chemistry

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10.1134/S1061934816040109

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Zherebker, A. Y., Perminova, I. V., Konstantinov, A. I., Volikov, A. B., Kostyukevich, Y. I., Kononikhin, A. S., & Nikolaev, E. N. (2016). Extraction of humic substances from fresh waters on solid-phase cartridges and their study by Fourier transform ion cyclotron resonance mass spectrometry. Journal of Analytical Chemistry, 71(4), 372-378. https://doi.org/10.1134/S1061934816040109

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title = "Extraction of humic substances from fresh waters on solid-phase cartridges and their study by Fourier transform ion cyclotron resonance mass spectrometry",

abstract = "Humic substances (HS) have been extracted from fresh waters on macroporous adsorbents of different types, Amberlite XAD-8 resin and Bond Elute PPL solid-phase cartridge. Comparative analysis of the extracted samples by ultra-high resolution mass spectrometry demonstrated selectivity of the selected adsorbents to the components of the molecular assembly of HS: the XAD-8 resin has affinity to the higher oxidized aromatic compounds and PPL has affinity to substances of stronger aliphatic character and nitrogen-containing compounds. Because of this fact, a comparison of the molecular composition of HS isolated from various sources must be performed taking into account selective adsorption; therefore, it is necessary to compare the products extracted by the same adsorbent for correct interpretation.",

keywords = "Fourier transform mass spectrometry, XAD-8, extraction, fresh water, humic substances, selective adsorption, solid-phase cartridge",

author = "Zherebker, {A. Ya} and Perminova, {I. V.} and Konstantinov, {A. I.} and Volikov, {A. B.} and Kostyukevich, {Yu I.} and Kononikhin, {A. S.} and Nikolaev, {E. N.}",

note = "Publisher Copyright: {\textcopyright} 2016, Pleiades Publishing, Ltd.",

year = "2016",

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day = "1",

doi = "10.1134/S1061934816040109",

language = "English",

volume = "71",

pages = "372--378",

journal = "Journal of Analytical Chemistry",

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publisher = "Pleiades Publishing",

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Zherebker, AY, Perminova, IV, Konstantinov, AI, Volikov, AB, Kostyukevich, YI, Kononikhin, AS & Nikolaev, EN 2016, 'Extraction of humic substances from fresh waters on solid-phase cartridges and their study by Fourier transform ion cyclotron resonance mass spectrometry', Journal of Analytical Chemistry, vol. 71, no. 4, pp. 372-378. https://doi.org/10.1134/S1061934816040109

TY - JOUR

T1 - Extraction of humic substances from fresh waters on solid-phase cartridges and their study by Fourier transform ion cyclotron resonance mass spectrometry

AU - Zherebker, A. Ya

AU - Perminova, I. V.

AU - Konstantinov, A. I.

AU - Volikov, A. B.

AU - Kostyukevich, Yu I.

AU - Kononikhin, A. S.

AU - Nikolaev, E. N.

PY - 2016/4/1

Y1 - 2016/4/1

N2 - Humic substances (HS) have been extracted from fresh waters on macroporous adsorbents of different types, Amberlite XAD-8 resin and Bond Elute PPL solid-phase cartridge. Comparative analysis of the extracted samples by ultra-high resolution mass spectrometry demonstrated selectivity of the selected adsorbents to the components of the molecular assembly of HS: the XAD-8 resin has affinity to the higher oxidized aromatic compounds and PPL has affinity to substances of stronger aliphatic character and nitrogen-containing compounds. Because of this fact, a comparison of the molecular composition of HS isolated from various sources must be performed taking into account selective adsorption; therefore, it is necessary to compare the products extracted by the same adsorbent for correct interpretation.

AB - Humic substances (HS) have been extracted from fresh waters on macroporous adsorbents of different types, Amberlite XAD-8 resin and Bond Elute PPL solid-phase cartridge. Comparative analysis of the extracted samples by ultra-high resolution mass spectrometry demonstrated selectivity of the selected adsorbents to the components of the molecular assembly of HS: the XAD-8 resin has affinity to the higher oxidized aromatic compounds and PPL has affinity to substances of stronger aliphatic character and nitrogen-containing compounds. Because of this fact, a comparison of the molecular composition of HS isolated from various sources must be performed taking into account selective adsorption; therefore, it is necessary to compare the products extracted by the same adsorbent for correct interpretation.

KW - Fourier transform mass spectrometry

KW - XAD-8

KW - extraction

KW - fresh water

KW - humic substances

KW - selective adsorption

KW - solid-phase cartridge

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U2 - 10.1134/S1061934816040109

DO - 10.1134/S1061934816040109

M3 - Article

AN - SCOPUS:84962737658

SN - 1061-9348

VL - 71

SP - 372

EP - 378

JO - Journal of Analytical Chemistry

JF - Journal of Analytical Chemistry

IS - 4

ER -

Extraction of humic substances from fresh waters on solid-phase cartridges and their study by Fourier transform ion cyclotron resonance mass spectrometry

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