Facile method for trimethylsilylation of alcohols using hexamethyldisilazane and ammonium thiocyanate under neutral conditions

Vrushali H. Jadhav; K. S.Ajish Kumar; Vinod D. Chaudhari; Dilip D. Dhavale

doi:10.1080/00397910701227440

Facile method for trimethylsilylation of alcohols using hexamethyldisilazane and ammonium thiocyanate under neutral conditions

Vrushali H. Jadhav
, K. S.Ajish Kumar
, Vinod D. Chaudhari
, Dilip D. Dhavale

Research output: Contribution to journal › Article › peer-review

15 Scopus citations

Abstract

A highly efficient method for trimethylsilylation of primary, secondary, tertiary, allylic, and a variety of sugar-derived alcohols using hexamethyldisilazane in the presence of a catalytic amount of ammonium thiocyanate under neutral conditions is reported.

Original language	English
Pages (from-to)	1363-1370
Number of pages	8
Journal	Synthetic Communications
Volume	37
Issue number	8
DOIs	https://doi.org/10.1080/00397910701227440
State	Published - 1 Jan 2007
Externally published	Yes

Keywords

1,1,1,3,3,3-hexamethyldisilazane
Alcohols
Ammonium thiocyanate
Trimethylsilylation

ASJC Scopus subject areas

Organic Chemistry

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10.1080/00397910701227440

Cite this

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title = "Facile method for trimethylsilylation of alcohols using hexamethyldisilazane and ammonium thiocyanate under neutral conditions",

abstract = "A highly efficient method for trimethylsilylation of primary, secondary, tertiary, allylic, and a variety of sugar-derived alcohols using hexamethyldisilazane in the presence of a catalytic amount of ammonium thiocyanate under neutral conditions is reported.",

keywords = "1,1,1,3,3,3-hexamethyldisilazane, Alcohols, Ammonium thiocyanate, Trimethylsilylation",

author = "Jadhav, \{Vrushali H.\} and Kumar, \{K. S.Ajish\} and Chaudhari, \{Vinod D.\} and Dhavale, \{Dilip D.\}",

year = "2007",

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doi = "10.1080/00397910701227440",

language = "English",

volume = "37",

pages = "1363--1370",

journal = "Synthetic Communications",

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TY - JOUR

T1 - Facile method for trimethylsilylation of alcohols using hexamethyldisilazane and ammonium thiocyanate under neutral conditions

AU - Jadhav, Vrushali H.

AU - Kumar, K. S.Ajish

AU - Chaudhari, Vinod D.

AU - Dhavale, Dilip D.

PY - 2007/1/1

Y1 - 2007/1/1

N2 - A highly efficient method for trimethylsilylation of primary, secondary, tertiary, allylic, and a variety of sugar-derived alcohols using hexamethyldisilazane in the presence of a catalytic amount of ammonium thiocyanate under neutral conditions is reported.

AB - A highly efficient method for trimethylsilylation of primary, secondary, tertiary, allylic, and a variety of sugar-derived alcohols using hexamethyldisilazane in the presence of a catalytic amount of ammonium thiocyanate under neutral conditions is reported.

KW - 1,1,1,3,3,3-hexamethyldisilazane

KW - Alcohols

KW - Ammonium thiocyanate

KW - Trimethylsilylation

UR - https://www.scopus.com/pages/publications/34247103221

U2 - 10.1080/00397910701227440

DO - 10.1080/00397910701227440

M3 - Article

AN - SCOPUS:34247103221

SN - 0039-7911

VL - 37

SP - 1363

EP - 1370

JO - Synthetic Communications

JF - Synthetic Communications

IS - 8

ER -

Facile method for trimethylsilylation of alcohols using hexamethyldisilazane and ammonium thiocyanate under neutral conditions

Abstract

Keywords

ASJC Scopus subject areas

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