Abstract
X-ray diffraction and electron microscopy have been used in an investigation of the shaping of phase composition and structure of a coprecipitated NiO-WO//3 system in calcination, reduction, and sulfiding. It has been shown that calcination, when it leads to the formation of crystalline NiWO//4, lowers the efficiency of reduction and sulfiding to a considerable degree. A step-temperature sulfiding operation, in comparison with isothermal sulfiding, gives a less ordered structure of the WS//2, with loose packing of the particles into agglomerates.
Original language | English |
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Pages (from-to) | 1042-1047 |
Number of pages | 6 |
Journal | Kinetics and Catalysis |
Volume | 26 |
Issue number | 5 pt 2 |
State | Published - 1 Sep 1985 |
Externally published | Yes |
ASJC Scopus subject areas
- Catalysis
- Chemistry (all)
- Modeling and Simulation
- Computer Science Applications