Reaction of dimethyl(chloromethyl)chlorosilane with trimethylsilyl derivatives of l-phenyl-2-acetyl- and 1-phenyl-2-trifluoroacetylhydrazines

I. D. Kalikhman; O. B. Bannikova; L. I. Volkova; L. I. Belousova; T. I. Yushmanova; V. A. Lopyrev; O. A. Vyazankina; N. S. Vyazankin; V. A. Pestunovich

doi:10.1007/BF01474219

Reaction of dimethyl(chloromethyl)chlorosilane with trimethylsilyl derivatives of l-phenyl-2-acetyl- and 1-phenyl-2-trifluoroacetylhydrazines

I. D. Kalikhman, O. B. Bannikova, L. I. Volkova, L. I. Belousova, T. I. Yushmanova, V. A. Lopyrev, O. A. Vyazankina, N. S. Vyazankin, V. A. Pestunovich

Research output: Contribution to journal › Article › peer-review

Abstract

The reaction of dimethyl(chloromethyl)chlorosilane with the phenylhydrazone of 1-triraethylsiloxyethanone proceeds with initial trans-silylation and subsequent formation of (O→ Si)-chloro[2-(1-phenyl-2-acetylhydrazino)methyl]diraethylsilane. The analogous reaction with the phenylhydrazone of 1-trimethylsiloxy-2-trifluoroethanone terminates at the trans-silylation step.

Original language	English
Pages (from-to)	2550-2551
Number of pages	2
Journal	Bulletin of the Academy of Sciences of the USSR Division of Chemical Science
Volume	35
Issue number	12
DOIs	https://doi.org/10.1007/BF01474219
State	Published - 1 Dec 1986
Externally published	Yes

ASJC Scopus subject areas

General Chemistry

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Kalikhman, I. D., Bannikova, O. B., Volkova, L. I., Belousova, L. I., Yushmanova, T. I., Lopyrev, V. A., Vyazankina, O. A., Vyazankin, N. S., & Pestunovich, V. A. (1986). Reaction of dimethyl(chloromethyl)chlorosilane with trimethylsilyl derivatives of l-phenyl-2-acetyl- and 1-phenyl-2-trifluoroacetylhydrazines. Bulletin of the Academy of Sciences of the USSR Division of Chemical Science, 35(12), 2550-2551. https://doi.org/10.1007/BF01474219

@article{074f1f7b8b814cc58407f5fa8480ebea,

title = "Reaction of dimethyl(chloromethyl)chlorosilane with trimethylsilyl derivatives of l-phenyl-2-acetyl- and 1-phenyl-2-trifluoroacetylhydrazines",

abstract = "The reaction of dimethyl(chloromethyl)chlorosilane with the phenylhydrazone of 1-triraethylsiloxyethanone proceeds with initial trans-silylation and subsequent formation of (O→ Si)-chloro[2-(1-phenyl-2-acetylhydrazino)methyl]diraethylsilane. The analogous reaction with the phenylhydrazone of 1-trimethylsiloxy-2-trifluoroethanone terminates at the trans-silylation step.",

author = "Kalikhman, {I. D.} and Bannikova, {O. B.} and Volkova, {L. I.} and Belousova, {L. I.} and Yushmanova, {T. I.} and Lopyrev, {V. A.} and Vyazankina, {O. A.} and Vyazankin, {N. S.} and Pestunovich, {V. A.}",

year = "1986",

month = dec,

day = "1",

doi = "10.1007/BF01474219",

language = "English",

volume = "35",

pages = "2550--2551",

journal = "Bulletin of the Academy of Sciences of the USSR Division of Chemical Science",

issn = "0568-5230",

publisher = "Springer New York",

number = "12",

}

Kalikhman, ID, Bannikova, OB, Volkova, LI, Belousova, LI, Yushmanova, TI, Lopyrev, VA, Vyazankina, OA, Vyazankin, NS & Pestunovich, VA 1986, 'Reaction of dimethyl(chloromethyl)chlorosilane with trimethylsilyl derivatives of l-phenyl-2-acetyl- and 1-phenyl-2-trifluoroacetylhydrazines', Bulletin of the Academy of Sciences of the USSR Division of Chemical Science, vol. 35, no. 12, pp. 2550-2551. https://doi.org/10.1007/BF01474219

Reaction of dimethyl(chloromethyl)chlorosilane with trimethylsilyl derivatives of l-phenyl-2-acetyl- and 1-phenyl-2-trifluoroacetylhydrazines. / Kalikhman, I. D.; Bannikova, O. B.; Volkova, L. I. et al.
In: Bulletin of the Academy of Sciences of the USSR Division of Chemical Science, Vol. 35, No. 12, 01.12.1986, p. 2550-2551.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - Reaction of dimethyl(chloromethyl)chlorosilane with trimethylsilyl derivatives of l-phenyl-2-acetyl- and 1-phenyl-2-trifluoroacetylhydrazines

AU - Kalikhman, I. D.

AU - Bannikova, O. B.

AU - Volkova, L. I.

AU - Belousova, L. I.

AU - Yushmanova, T. I.

AU - Lopyrev, V. A.

AU - Vyazankina, O. A.

AU - Vyazankin, N. S.

AU - Pestunovich, V. A.

PY - 1986/12/1

Y1 - 1986/12/1

N2 - The reaction of dimethyl(chloromethyl)chlorosilane with the phenylhydrazone of 1-triraethylsiloxyethanone proceeds with initial trans-silylation and subsequent formation of (O→ Si)-chloro[2-(1-phenyl-2-acetylhydrazino)methyl]diraethylsilane. The analogous reaction with the phenylhydrazone of 1-trimethylsiloxy-2-trifluoroethanone terminates at the trans-silylation step.

AB - The reaction of dimethyl(chloromethyl)chlorosilane with the phenylhydrazone of 1-triraethylsiloxyethanone proceeds with initial trans-silylation and subsequent formation of (O→ Si)-chloro[2-(1-phenyl-2-acetylhydrazino)methyl]diraethylsilane. The analogous reaction with the phenylhydrazone of 1-trimethylsiloxy-2-trifluoroethanone terminates at the trans-silylation step.

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DO - 10.1007/BF01474219

M3 - Article

AN - SCOPUS:34250122568

SN - 0568-5230

VL - 35

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EP - 2551

JO - Bulletin of the Academy of Sciences of the USSR Division of Chemical Science

JF - Bulletin of the Academy of Sciences of the USSR Division of Chemical Science

IS - 12

ER -

Reaction of dimethyl(chloromethyl)chlorosilane with trimethylsilyl derivatives of l-phenyl-2-acetyl- and 1-phenyl-2-trifluoroacetylhydrazines

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